青云英语翻译

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a将(Ⅱ)(g, 0.1mol)充分溶解于THF中,用导针将溶液导入加有镁屑(12g, 0.5mol)的烧瓶中,并用一颗碘粒引发格氏反应。滴液完毕后将水浴温度调至THF回流并反应两小时。反应完毕后将溶液导入另一烧瓶,滴加二甲基氯硅烷(ml, 0.15mol)。常温搅拌过夜。反应加水终止。加入乙醚分液,水层继续用乙醚洗涤,合并油层后用旋蒸蒸去溶剂,用正己烷作为展开剂过柱分离。蒸去展开剂,得Ⅲ( g, mol), 收率 %. (Ⅱ) (g, 0.1mol) the full dissolution in THF, inducts with the guide stem the solution Canada has the magnesium filings (12g, 0.5mol) in the flask, and responded with idodine grain of initiation standard.After the dropping liquid finished transfers to the water bath temperature the THF backflow and r [translate] 
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